Volume 22 Issue 5

Published: 2025-06-25

Contents


Article
Spectrophotometric Determination of Metoclopramide Hydrochloride in Pharmaceutical Preparations UsingDiazotization Reaction

Kasim M. Al-Abbasi, Salim A. Mohammed, Lamya A. Sarsam,

A simple, rapid and sensitive spectrophotometric method has been developed for the quantitative determination of metoclopramide hydrochloride in both pure form and in its pharmaceutical...

DOI: 10.33899/rjs.2011.6509

Pages: 76-88
Synthesis of some Aryl sulfonamide Compounds from o-Nitrotoluene

Amera M. Farage, Asmaa H. Sultan, Mohammed A. Sheat,

2-Nitro-4-Methyl benzene sulphonyl chloride (I) has been prepared through sulphonation reaction from chlorosulphonic acid and o-nitrotoluene. Then compound (I) was allowed to react with primary and...

DOI: 10.33899/rjs.2011.6521

Pages: 57-61
The Effect of Tramadol on the Peristaltic Movement Small Intestine in Rabbit

Mohammad Y. AL-Fathee, Ghada A. Taqa, Maha K. AL- Jameel

Tramadol is an opium analgesic drug that is used to relieve moderate to relatively severe pain. The major side effect of opium analgesic drugs is inhibit the intestinal peristalsis motility, and...

DOI: 10.33899/rjs.2011.6516

Pages: 1-10
Antibacterial Activity of Water and Alcoholic Crude Extract of Flower Achillea millefolium

Rasha N. Hasson,

The aim of this study was to determine the antimicrobial effect of yarrow and it is flower extract on certain microorganisms. The ethanolic (alcoholic) extract of the flower and aqueous (water)...

DOI: 10.33899/rjs.2011.6518

Pages: 11-20
Conductivity Study of Tetra Aqua -1,10- Phenanthroline Zinc(II) Chloride in Aqueous Methanol Mixture at Different Temperatures

Firas A. Thanon,

The electrical behavior of association phenomena of tetra aqua (1,10 _ phenanthroline) zinc(II) chloride in methanol-water mixture have been investigated by precise conductance measurements at...

DOI: 10.33899/rjs.2011.6524

Pages: 98-107
Spectrophotometric Determination of Sodium Nitroprusside by Coupling with Diazotized p-Nitroaniline and Determination of Thermodynamic Parameters

Hayfa M. Jassim, Batool B. Ibraheem, Kasim Y. Rahawi,

The coupling reaction of sodium nitroprusside (SNP) with diazotized p-nitroaniline (DPNA) in basic media has been studied using spectrophotometric method. The intense yellow water-soluble...

DOI: 10.33899/rjs.2011.6525

Pages: 119-128
Synthesis and Characterization of Mn(II), Co(II), Ni(II),Cu(II), Zn(II) and Cd(II) Complexes with Thiophene -2- CarboxylicAcid Hydrazide

Ibraheem A. Al-Qassar, Abdul-Ghany M. Al- Daher,

Metal (II) complex of thiophene -2- carboxylic acid Hydrazide (TCH) ligand of the type [M(TCH)2X2] where M= Mn(II), Co(II), Ni(II),Cu(II), Zn(II) and Cd(II) , X=Cl-, NO3- have been prepared and...

DOI: 10.33899/rjs.2011.6513

Pages: 108-118
Spectrophotometric and High Performance Liquid Chromatographic Methods for Determination of Metoclopramide inPharmaceutical Preparations

Nada A. Khaleel, Hana Sh. Mahmood, Nabeel S. Othman,

A rapid, simple, and sensitive spectrophotometric and high performance liquid chromatographic methods have been developed for the quantitative determination of metoclopramide hydrochloride MCP in...

DOI: 10.33899/rjs.2011.6510

Pages: 39-56
Synthesis of some Derivatives 2-Aryl -1,3,4-Thiadiazoline-2-One

Salim J. Mohammad,

To synthesis of some new heterocyclic compounds containing 1,3,4-thiadiazole moieties. Many of 5-alkyl-3-(4-substituted-2-butyn-1-yl) -1,3,4-thiadaizoline-2(3H)-one (15a-e and 16a-e) have been...

DOI: 10.33899/rjs.2011.30512

Pages: 89-97
The Use of 3-Benzylidene Phthalide as Precursor to Synthesize New 1,3,4-Oxadiazole Derivatives

Shaymaa K. Younis,

A series of new 2,5-disubstituted 1,3,4-oxadiazoles represented by compounds 2-phenyl-1-(2-(5-(5-aryl-1,3,4-oxadiazol-2-yl amino)-4H-1,2,4-triazol-3-yl)phenyl)ethanone (5a-f) have been synthesized...

DOI: 10.33899/rjs.2011.6507

Pages: 62-75
The Use of 3-Bezylidene Phthalide as Synthon in Synthesis of Heterocyclic Compounds

Shaymaa K. Younis,

2-(-Phenylacetyl) benzohydrazide (1) was prepared through the reaction of (Z)-3-benzylidene phthalide and hydrazine hydrate. Treatment of compound (1) with substituted benzoyl chloride yielded...

DOI: 10.33899/rjs.2011.6527

Pages: 21-38