Volume 26 Issue 5
Published: 2013-12-01
Contents
Article
Synthesis and Antibacterial Evaluation of Some 1,2,3-Selenadiazole Derivatives
Khalid M. Daoud, Mohanad Y. Saleh
Abstract In this paper the synthesis of some 1,2,3-Selenadiazoles derivative is reported . Acetophenone (A) , Cyclohexanone (B) and menthone (C) each was treated with p-toluensulfoyl hydrazide in...
DOI: 10.33899/edusj.2013.163051
Research Paper
Synthesis and diagnosis of a number of new binary zinc complexes with a mixture of lindane (derived from acetyl acetone and semicarbazone) and the study of bio-effectiveness and the effect of laser radiation on them
Zohoor Fathi Al-Tai, Aws Mohammed Alazi
Acetylacetoneazineoxime {AAOH}, acetylacetoneazinebis(oxime) {AABOH2}, benzilsemicarbazone {BScH} and benzilsemicarbazone hydrazone {BScZH} have been prepared using classical, one pot and microwave...
DOI: 10.33899/edusj.2013.163092
Determination of vanadium in Natural gas using graphite furnace atomic absorption spectrometry (GFAAS)
Suham Tawfiq, Abdul Majeed Khursheed, Tuana Khalil Abdulla
ABSTRACT Vanadium is recognized worldwide as the most abundant metallic constituent in petroleum, and this led to expect of its existing in natural gas that associated with oil as a trace amount in...
DOI: 10.33899/edusj.2013.163056
Spectrophotometric determination of chloramphenicol (after reduction) by nitrogen and conjugation using fluorochlosinol reagent - application to eye drops
Waadallah Bashir, Tamador Abbas Hamoudi
ABSTRACT A spectrophotometric method for the assay of micro amounts of chloramphenicol was developed. This method is based on the reduction of the nitro-group of chloramphenicol to amino-group,...
DOI: 10.33899/edusj.2013.163096
Preparation of activated carbon from asphalt and asphalt treated with polymers using microwave radiation
Khalid Owaid, Ahmed Ali Hammadi
ABSTRACT The study included the use of two path in the process of preparation.The first pathway included preparation of the AC from Baiji asphalt by an oxidation process done at 350 C using 2%...
DOI: 10.33899/edusj.2013.163100
Effect of Oral Contraceptive on some Serum Biochemical Parameters
Thana Y. Al-Obedy, Saba Al-Abachi
ABSTRACT The present study were aimed to determine the level of some biochemical parameters: (alkaline phosphatase ALP, creatine kinase CK, aspartate aminotranferase AST, urea, total bilirubin,...
DOI: 10.33899/edusj.2013.163068
Spectrophotometric Assay of Phenylephrine hydrochloride in Pharmaceutical Formulation with Alizarin Red sulphonate in Aqueous Solution
Thabit Saeed Al-Ghabsha, A. M.S. Al-Delymi
ABSTRACT A simple, rapid and sensitive spectrophotometric method for the determination of phenylephrine hydrochloride was developed. The method is based on the proton transfer reaction with...
DOI: 10.33899/edusj.2013.163054
Study of some thermal properties and activation energy of epoxy resin alloys with copper complex of acid N, N-5,2-toluene di-malic acid
Iptihag Zaki Al-Halim, Akram Aziz Mohammed
ABSTRACT Research includes the study of thermal isothermal Epoxy resin alloy with copper complex,( N,N - 2,5 Tolylene bismaleamic acid Copper (2,5TBMA Cu), through thermal analysis measurements...
DOI: 10.33899/edusj.2013.163105
Effect of Fructo-oligosaccharides and Xylo-oligosaccharaide (XO) assisted biotreatment on serum lipid concentrations in mice
Bilal Ahmed Saleh, Ahmed Talal Hikmat, Khalil Ibrahim Khalil
ABSTRACT The study was investigated the ability of prebiotics in reducing the lipids concentrations in the host where used laboratory mice for this purpose. The study included giving the laboratory...
DOI: 10.33899/edusj.2013.163104
Synthesis of some new heterocyclic compounds derived from 2-Chloro-3-formyl quinoline
Ala I. Ayoob, Fatma N. Mohmood
ABSTRACT In this paper the Synthesis of some substituted 2-Chloro-3-formyl quinoline (2ad) by treating various substituted acetanilide or 1-(4-substituted phenyl) ethanone oxime with POCl3 in...
DOI: 10.33899/edusj.2013.163057
Five-Membered Heterocyclic Ring Via Dichalcones
N. Ahmad, O Ali
ABSTRACT In this study some of dichalcone compounds (4-12) were prepared by the reaction of benzalacetone and its derivatives with a number of different ketones (acetophenone, acetanilide,...
DOI: 10.33899/edusj.2013.163064
Study of the inhibitory effect of some thiourea compounds on the activity of enzyme purified polyamine oxidase from the blood of patients with type 1 diabetes
Nashwan Ibrahim Abbou, Khawla Al.Fleih, Eyad Saadi Hamid
ABSTRACT The research included determination of polyamine oxidase (PAO) activity in normal and diabeti patients type I females. It was found that the activity of PAO in red blood cells (RBC) and...
DOI: 10.33899/edusj.2013.163091
Ultrasound Assisted Synthesis Of Pyrazolone Derivatives
Badie Ahmed, Jasim Abdullah
ABSTRACT The diazonium salt of 4-amino-1,5-dimethyl-2-phenyl-1H-pyrazol- 2-one (4-aminoantipyrine) was coupled with ethylacetoacetate and ethyl benzoylacetate to give the corresponding diazo...
DOI: 10.33899/edusj.2013.163055
Spectrophotometric determination of a number of aliphatic amines in aqueous solution and application to some pharmaceutical preparations
Thabet Saeed Ghabsha, Yousry Ibrahim Al-Nuaimi
ABSTRACT A simple , rapid and sensitive spectrophotometric method for the determination of aliphatic amines was developed .The method is based on the proton transfer reaction using 3,5-...
DOI: 10.33899/edusj.2013.163076
Preparation of palladium catalyst loaded on zeolite and its application in qualitative improvement of heavy naphtha
Omar Moussa Ramadan, Ragheed Ghazal, Kedar Salem Gargees
ABSTRACT In this research the catalyst palladium supported zeolite was prepared then X-ray diffraction and fluorescence and thermo gravimetric analysis was measured to understand the crystal and...
DOI: 10.33899/edusj.2013.163093
Estimation of lead and some biochemical variables in the blood of Al-Qayyarah refinery workers
Naoufel Shit Shahouth
ABSTRACT The study included measuring the concentration of lead in the blood of workers in the refinery Qayara and its effect on biochemical variables biochemical (such as glucose, cholesterol,...
DOI: 10.33899/edusj.2013.163095
Synthesis and characterization of Fe(II),Co(II),Ni(II),Cu(II) and Zn(II) complexes with Hexaaza macromolecule Ligands Derived from Semicarbazide
Saad K. Dawood, Falah Fakhree
ABSTRACT A new ligands( 3,4,6,14,15,17,23,24-Octaazatricyclo [17.3.1.18,12] tetracosa-1(23),8(24),9,11, 19 ,21- hexaene - 2,5,7,13,16,18 hexaone), (L1) and 2-(5-hydroxypentanoyl)...
DOI: 10.33899/edusj.2013.163067
Ultrasound-assisted one-pot synthesis of dihydropyrimid-2-one/thiones catalyzed by zirconyl chloride hexahydrate
Omar M. Yahya, Badie A. Ahmed, Imad Thanoon
ABSTRACT Different substituted dihydropyrimidinones and dihydropyrimidin thiones were generated from the Biginelli reaction between aromatic aldehydes, 1,3-dicarbonyl and urea or thiourea under...
DOI: 10.33899/edusj.2013.163065
Effect of Cyclosporine on the Relevant Biochemical Parameters in Renal Transplantation Patients in Mosul/Iraq
Suad Yousif Alkass, Shehab Yousif, Mohammed Fathel Hamid, Alaa Alhamadany
ABSTRACT Cyclosporine (sandimmune) is the backbone of immunosuppression in renal transplantation. However, it leads to multiple side effects, most of which are dose-dependent. In this respect, the...
DOI: 10.33899/edusj.2013.163070
Synthesis and Biological evalution of some substituted 2-dibenzyl amino 1,3,4-oxadiazoles , thiadiazoles and 1,2,4-triazoles
Khalid Mahmood Daoud, Shaima S. Ismmaeel
ABSTRACT In this paper the synthesis of some substituted 2-dibenzyl 1,3,4-oxadiazole, thiadiazole and 1,2,4-triazoles derived from dibenzyl amine is reported scheme-1. Dibenzyl amine was treated...
DOI: 10.33899/edusj.2013.163061
Synthesis of Some Heterocyclic Compounds Containing Tetrahydroisoquinoline Moiety
Mohammad Ahmad Al-Iraqi, Ahmad Waleed Najem
ABSTRACT This research involves synthesis of some five membered heterocyclic compounds using 1,2,3,4-tetrahydroisoquinoline as a synthone. The initial step in this research involves the reaction...
DOI: 10.33899/edusj.2013.163063
Partial purification and study of kinetic enzyme reductase in blood cell decomposition of mice with induced atherosclerosis and inhibitory effect of some isoflavones.
Nahida Aljalabe, Eman Saeed Aljoga
ABSTRACT The reseach includes isolation and study some kinetic characteristics of aldose reductase (AR2) from blood cells hemolysate for miceinduced atherosclerosis and normal mice. Two peaks of...
DOI: 10.33899/edusj.2013.163075
The use of dipron coupling reagent in the spectrophotometric determination of aniline in presence of Sodium metaperiodate in aqueous solution
Ilham Saad Allah AlTalbi, Maysam Hossam ALFakhry
ABSTRACT A simple rapid and specific method was developed for the determination of aniline .The method depends on the organic oxidative coupling reaction of dipyrone (metamizole sodium) with...
DOI: 10.33899/edusj.2013.163110
Spectrophotometric Assay of Bromhexine hydrochloride in Pure and in Pharmaceutical Dosage Forms by Diazometry Coupling Reaction
Salim A. Mohammed, Rana F. Almukhtar
ABSTRACT Asimple, accurate and sensitive spectrophotometric method has been developed for quantitative determination of bromhexine hydrochloride (BH) in both pure form and in its pharmaceutical...
DOI: 10.33899/edusj.2013.163069
Synthesis , Characterization of Some Benzilyl Hydrazone Derived from Benzilic Acid Hydrazide
Salim A. Mohammed, Fatin G. zuhair
(4a-g)(5a-f) , ,
DOI: 10.33899/edusj.2013.163072
Microwave-assisted Degradation of Polyvinyl Chloride Induced by Complexes of Transition Elements
Tariq Abdul-Jaleel, Hameed Ali, Ahmad Obeed
ABSTRACT In this work, the presence of variable metals complex of [N,N-Bis(Salicylidene)1,2-[diaminoethane] Nickel(II), (Ni-BSEDA). And the PVC film were studied under the microwave radiation. The...
DOI: 10.33899/edusj.2013.163073
The relationship of the lipoxygenase enzyme in female blood with cardiovascular diseases
Amira Aziz Mahmoud, Rawia Rashed
ABSTRACT Lipoxygenase , LOX, is one of the enzymes that affect the lipid metabolism. On the other hand, lipids can influence the risk of cardiovascular diseases and diabetes. Therefore, the...
DOI: 10.33899/edusj.2013.163099
Study of Alkaline phosphatase Inhibition by theophylline and trifluoperazine in vitro
Bilal Jasir Alrawi, Khalid Farooq Alrawi, Shakir Mahmood Alfahdawi
ABSTRACT The aim of this research is to study the inhibition effect of theophylline and trifluoperazine in vitro on alkaline phosphatase and determine the type of inhibitions. A series of...
DOI: 10.33899/edusj.2013.163062
Preparation of a number of heterocyclic compounds derived from benzotrazole
Mohamed Khedr Mohamed, Ahmed Khedr Ahmed
ABSTRACT In this thesis, a number of heterocyclic compounds with five-memberd , such as substituted oxadiazole , thiadiazole , pyrazole , iso andoline-1,3-dione , also the preparation of pyrroline...
DOI: 10.33899/edusj.2013.163097
Preparation of activated carbon from a mixture (wood _ polymer) using microwave radiation
Mayada Mahmood Ali, Khalid ِAhmed Owaid, Ahmed Abdul Karim Thanoon
ABSTRACT The research work was aimed for preparation of activated carbon from blending the wood of lead tree with variable ratio of polymers organic glass(PMMA),recycled rubber (5,10,15)% after...
DOI: 10.33899/edusj.2013.163078
Synthesis and Characterization of Mn(II) ,Co(II) ,Ni(II) ,Cu(II) ,Zn(II) and Cd(II) Complexes with Di-Schiff Bases Derived from o- or m- Phenylenediamine and 9,10-Phenanthrenequinone
K. Al-Nama, A. Abdullah
ABSTRACT Aseries of new complexes of the type [MLCl2] where M=Mn (II),Co(II),Ni(II),Cu(II),Zn(II),Cd(II) L=L1 or L2 represents di- Schiff base ligands:...
DOI: 10.33899/edusj.2013.163059
Study of the properties and inhibition of the polyamine oxidase enzyme partially purified from the fruit of green pepper by amyloride and medovi
Wathba Idris Touhala, Muheeb Mohammed Jassim
ABSTRACT The study included a detection of PAO in green pepper (Capsicum grossum) and its partial purification by using dialysis and anion exchange chromatography (using DEAE cellulose) techniques...
DOI: 10.33899/edusj.2013.163101
Synthesis and characterization Studies of Mixed Ligand (1,3,4-oxadiazole derivative and ethylenediamine or acetylacetone)complexes with Ni(II)
Rezhna Faraj, Hikmat Mohamad
ABSTRACT This work includes the synthesis of the ligands (POTL = 5-Phenyl-1,3,4-oxadiazole-2-thiol , NPOTL = 5-(3-Nitro-phenyl)-1,3,4-oxadiazole-2-thiol , and NPOTE =...
DOI: 10.33899/edusj.2013.163066
Spectroscopic and Fluorometric Determination of Cinnarizine and Dipyridamole in Pharmaceutical Tablets Using Eosin Y Dye
Zeina Zuhair Al - Abdali, Elham Saad Allah Saleh
ABSTRACT Spectrophotometric and spectrofluorimetric methods were developed for the determination of cinnarizine and dipyridamole. The spectrophotometric method is based on the formation of ion pair...
DOI: 10.33899/edusj.2013.163098
Preparation of a number of 4,3,1-oxadiazole substituted derived from imidazole and evaluation of their biological effectiveness
Khaled Al Badrani, Khalid Matni Al-Janabi, Ammar Saad Eddin
ABSTRACT Ethyl 2-(1H-imidazol-1-yl)acetate (A1) was synthesized by the reaction of ethylchloroacetate with imidazol, Then refluxed with hydrazine hydrate to obtain 2-(1H-imidazol-1-yl)acidhydrazid...
DOI: 10.33899/edusj.2013.163107
Study on recycling and characterization of some waste polymers
Hiba M. Awad, Fawzi habeeb Jabrail
ABSTRACT Chemical recycling of waste polymers is one of the important recent objective.The wastepolyethelene that present in two structures (LDPE&HDPE),beside waste polypropylene ,polystyrene...
DOI: 10.33899/edusj.2013.163071
A study of multisubstituted chain transfer agents on the kinetics of homopolymerisation of methylmethacrylate .
Dhari M. Abdullah
ABSTRACT : A continuation to a previous study of monosubstiuted transfer agents, carried out by the same author, this investigation had been done. It has been found that multisubstituted chain...
DOI: 10.33899/edusj.2013.163074
Synthesis and Study of New Complexes of a Mixture of Liquandate for Schiff Bases Derived from Isatin and Amino Acids and Bi-Amine Liquandate with Iron Ion (II)
Khalaf Ibrahim Khaloo, Abeer Salim Al Nuaimi
ABSTRACT The work includes the synthesis and characterization of new complexes of mixed ligands of Schiff bases derived from isatin with amino acids...
DOI: 10.33899/edusj.2013.163094
Synthesis of Some New Amides Derived from Indomethacin
Kawther Al-Naimi, Haitham A. Alwahb, Hyffaa younis
ABSTRACT Indomethacin (1) was alb wed to react with thionyl chloride in dry benzene to yield [1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl chloride (2) which was readily converted...
DOI: 10.33899/edusj.2013.163060
Synthesis and diagnosis of a number of new super oxo compounds derived from Schiff base complexes for dual cobalt
Saad El Mokhtar, Tamador Mahmoud, Lana Rashid
ABSTRACT: The work included the preparation of cobalt complexes having general formula [ CoL] , where L is divalent tetradentate Schiff base ligand derived from benzyl and anthranilic acid or...
DOI: 10.33899/edusj.2013.163077
The Effect of Age, Smoking and Exercise on Sorbitol Dehydrogenase and its Correlation Factor with Some Biochemical Variables in Diabetics
Wasan Khairallah Ali, Maher Abdul Sattar Al - Dabbagh
ABSTRACT This research includes a biochemical study of sorbitol dehydrogenase (SDH) in the serum of the control and patient with diabetes mellitus. Their ages ranged between (8-65year) . It has...
DOI: 10.33899/edusj.2013.163103
Synthesis, Diagnosis and Study of Natural Nano-Silica Complexes with Polyester Razin and Polystyrene - Butadiene
Tareq Abdul Jalil Mandil, Mohammad Abd Al Kareem
ABSTRACT For the preparation of composite materials environ mentally friendly natural nano particle silica derived from rice husks has as streng thening of Iraqi natural materials in a ratio of(2,...
DOI: 10.33899/edusj.2013.163106
Relationship of zinc, copper and manganese levels on bone formation that increases the risk of uterine cancer
Zeina Abdel Moneim Al - Jawadi, Zainab Mahfouz Al Nuaimi
ABSTRACT: Due to the lack of previous studies on the impact of osteoporosis on the incidence of uterine cancer, and the rapid spread of uterine cancer in recent years all over the world, and the...
DOI: 10.33899/edusj.2013.163102
Preparation of poly (acro-yellow hydroxamic acid) from the polymer (methyl acrylate) and study use it in the water purification from heavy metal elements.
Saddaa Abd Abdullah Gamal
ABSTRACT The aim of this research is the preparation of Poly (Methylacrylate) by a free radical initiating process for polymerization methyacrylate using benzoyl peroxide as an intiator at (70C )...
DOI: 10.33899/edusj.2013.163109
Spectrophotometric Method for Determination of Chloramphenicol in Pharmaceutical Preparations using o-Chloranil Reagent
Thabit Saeed Al-Ghabsha, Theiaa Al-Sabha, Mohammed Al-Enizzi
. - 527 . 2-65 / 3.72310 .-1-1 . 0.456 1.521 / 100.9% 2.2%. . . .
DOI: 10.33899/edusj.2013.163053
A spectrophotometric micro determination of pyridoxine hydrochloride by coupling diazometry
Mohammad Saleem Saleem, Zaheda Ahmad Mohammed
ABSTRACT A simple, rapid and sensitive spectrophotometric method has been investigated for determination of microgram amount of pyridoxine hydrochloride .The method is based on the oxidation of...
DOI: 10.33899/edusj.2013.163052
Construction of a selective membrane electrode for the determination of procaine hydrochloride by Schiff bases
Siham Tawfiq Amin, Faiz Mohsin Hamid, Obaid Abdullah Jassim
ABSTRACT This project including synthesis of selective membrane electrode ,consisting of electrically active material produced from Schiff base reaction of (procaine hydrochloride , m-hydroxyl...
DOI: 10.33899/edusj.2013.163079
Synthesis and Characterization of Ruthenium (III) Complexes with Substituted Nitrones
Khalaf Ibrahim Khallow, Eman M.H. Al-Bayate
ABSTRACT New series of complexes of general [Ru(Cl)2(H2O)2.L]nH2O ; where LH=[-(2-hydroxy-1-naphthyl)-N-(p-R-phenyl nitrone] n=0-6 and R=H, Cl , Br , COCH3 , NHCOCH3 , NH2 and CH3 were formula...
DOI: 10.33899/edusj.2013.163058
Comparison of pKa values for some phenols imines derived from 3-acetyl and 4-acetyl pyridines.
Adel S. Azzouz, R .D.S. Uezbaky
Abstract The study includes the preparation of a new six imines derived from the mother ketones, namely the 3-acetyl and 4-acetyl pyridines. These imines containing phenols groups in ortho, meta...
DOI: 10.33899/edusj.2013.163050
